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1 article(s) from Stollenz, Michael

Non-metal-templated approaches to bis(borane) derivatives of macrocyclic dibridgehead diphosphines via alkene metathesis

Tobias Fiedler,
Michał Barbasiewicz,
Michael Stollenz and
John A. Gladysz

Beilstein J. Org. Chem. 2018, 14, 2354–2365, doi:10.3762/bjoc.14.211

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Scheme 1: Syntheses of gyroscope like platinum and rhodium complexes and dibridgehead diphosphines derived th...

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Scheme 2: Synthesis and alkene metathesis of the monophosphorus precursor 1·BH₃.

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Figure 1: The ¹³C{¹H} NMR spectra (CDCl₃, 100 MHz) of in,out-2·2BH₃, (in,in/out,out)-2·2BH₃, 6·2BH₃, and the ...

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Scheme 3: Synthesis of the diphosphorus precursor 11·2BH₃.

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Scheme 4: Truncated approaches to the diphosphorus precursor 11·2BH₃ from 10.

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Scheme 5: Alkene metathesis of the diphosphorus precursor 11·2BH₃.

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Scheme 6: Schematic comparison of the key alkene metathesis steps in Scheme 2 and Scheme 5.

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Scheme 7: Steps that set the in,in/out,out vs in,out stereochemistry of 2·2BH₃ in Scheme 2 and Scheme 5.

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Scheme 8: Another non-metal-templated approach to dibridgehead diphosphorus compounds.

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Scheme 9: Previously synthesized dibridgehead diphosphine diboranes.

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Scheme 10: Alkene metathesis of the tetraalkenyldiphosphine diborane 19·2BH₃.

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Published 07 Sep 2018

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